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Front Physiol 9:44

Bubber, P., Hartounian, V., Gibson, G

If a peptide has not dissolved after 30 minutes of gentle periodic swirling, there may be a solubility issue, and you should consider using a different solvent or adding more water

The use of CO for diagnostic purposes, such as total haemoglobin mass measurements or the determination of pulmonary diffusion capacity, is not prohibited